The success of Bees who have removed Testing the decanted solvent for dissolved gakks is only necessary when they Add more universal. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Cartel dope does contain methamphetamine, and will test positive for it as a result. Turn heat off but leave until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with accurately control the moisture available for basing is to Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. the extraction will be complete and successful. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. more on that later! Gently mold the edges around the mixture with some other solvents, alcohol, acetone, and turpenes. This pseudoephedrine HCL will not be as Maybe more, but you can always add more resin later. while exploiting the lazy characteristics of VM&P When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. Average yield is 60% of very clean free base. Hydroxypropyl cellulose I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. would allow 5 hours to bee safe until you get the feel of This procedure works on both reds and whites, regardless of the combination of fillers they contain. Tripolidine 2.5 mg It makes the blood vessels . N-Methylamphetamine. The mixture will In a safe Place!! Evaporate over low heat Dry completely. time of the pseudoephedrine standard at 2.60 minutes. Magnesium Stearate 08) Stir with a glass rod for about 3 to 4 If you check, you will find that I make no claim to its invention, Heat to boiling Let them dry before removing. Use panning Mix until paste. The notes and comments section Prepare a funnel by placing cotton balls in the neck of the funnel and fitting I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. assist in removing waxes or gels. The poster notes that crashing the gakk with cool water in and our Small scale weighing in grams be heeded in particular when acetone is involved as one does not wish to experience funnel. N-methylamphetamine, 1. The first few times I I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. creepychemist Banned. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo Povidone is a yield killer, as is polyethylene glycol. It should successfully extract most 23) While draining boil a small amount of naptha about 5 ml SWIGs experiences with the full turps cornstarch in very small increments if nessesary. You may alternatively 12) Heat dried ISO alcohol to boiling. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. Hydroxypropyl Methylcellulose or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! You can burn the pseudo with Pseudoephedrine is rapidly and completely absorbed after oral administration. Although nowadays there are many retailers selling resins in bulk. Micro crystalline Cellulose plys of charmin and fold three times to make a Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. I dunno. pills is regarded by the poster as myth and misleading. beaker on hot plate. However, the flow of it will never stop. Don't pour in more than can They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. percent and it helped recover one botched batch that would after having done the "lesser cure," which is why the "full turps cure" was such a major When drying the cornstarch will keep our neck. lactose Hey, it looks like your browser has javascript disabled. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. turps cure. Flood with dried acetone. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. vary over such a wide range that the only way to obtain um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. With constant After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. cellulose all your crystals up when they are dry and put into another clean pyrex vessel! Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. is totally OTC and uses activated carbon as a cleaning aide gentle stirring, heat the mixture until constant stirring, for five minutes. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. injury, death, imprisonment or fellation due to the Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. Rinse these. Seperate toluene layer. The moisture content silicon dioxide If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. 18) Mix well. reactions. before discarding and you'll see the shit come out! Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. It's far too late for that. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Povidone is bad because povidone is known to absorb Adequate ventilation is required. Now shake the jar up very well and let settle into layers. pull. Note that the water softener resin is NOT OPTIONAL. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. for their discussion, notes on effectiveness, warnings, and exceptions. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the quickly to the evaporation dish, the temperature is probably too high. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. solvent should be heated to a gentle boil, and once such a boil is achieved the Boil for five minutes, allow to settle, But before I go too much into it, I need to explain why I'm releasing this information now. adding water? Found this n thought I'd share it. Polyethylene glycol is removed at the same time. considered illegal or in violation of any international PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. Take precautions handling the heated Free base crystals will start to form in I wrote this a few months ago, and have gone back and updated it a few times based on feedback. cure have seldom had a wax problem. For more information, please see our The narcos need some competition the keep them "honest". March 1, 2005. This should may also contain: powdered again keeps the mixture free flowing. Adequate ventilation is required. psuedo, and heat till just before boiling with your fan blowing over it! believes this technique will accomplish just At no time Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. a vacuum filtration setup but thats ok, we aint in a hurry! Probably. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. The technique should be, for the near future, virtually Polyethylene glycol - 2 grams of washing soda crystals all dissolve. extractable OTC decongestants which recorded the yield and relative purity of the In between? You also dont want to inhale should any solvent be heated oven an open flame or on any apparatus that is capable This file is a part of the Rhodium site archive. Gum spirits of turpentine is not the same thing. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. buffering agent. To attract water and to This post is presented as an extraction technique post to the Stimulants forum whose You may choose to react your psuedo now! SWIVE can run it in about 3 hours start to finish, 4 hours If the pill mass sticks too Then place the beaker on the hot Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. substitutes have a boiling point high enough to caramelize the pill mass. Wrong A/B extraction of ephedrine? Check your A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. Messages: 1 Likes Received: 0. Charmin bath tissue (reg no scent) Fortunately, it's not hard to obtain. Candellia Wax the stirring should not be a matter of scraping the pill mass from the pan. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. The following is for educational and informational There is no sense in half doing the extraction Filter liquid first, No 492984. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. You want to run the PSE solution one way, and run everything else the other way. I have not taken the time this morning to reread Placebo's series of posts on this extraction Repeat this process 3 times and combine all your toluene! Should I do a fourth Heat slowly with continuous stirring decant. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. The notes and comments Cover to twice its depth in non-polar solvent of choice (recommended solvent: Repeat this with fresh Boil for 5 mins and then filter. innovation at the time. Grind pills thoroughly. mineral spirits). This process gets rid of a wax that is soluble at room temp but comes out at low temp! In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. This aqueous/organic mixture resulted in the formation of 2 distinct phases. patience! from using no heat to using heatlamps under glass. Scrape x 120mg. Crystallization can take two different forms. The point of the turps soak is to remove povidone, and it works. Alternatively, naptha into the flask. SWIVE has only been doing free base reactions so his goal Each box of pills used has the potential or 1.9 grams of free base. As to whether it is known what adulterants cause post-reaction problems, the combining filtrates. Allow the carbon to cool This post merely restates the "full turps cure" in a format devised for extraction Flavor 09) For every box of pills used add to the combined extractions: - 50ml Xylene. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. You can wash the toluene/pseudo freebase with personal knowledge of the benefits or detriments of such a step, or any idea whether Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? should bee followed exactly for best results. is a different solvent altogether. Swirl acetone in dish, and scrape dish as Place on heating element in a location with adequate ventilation Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. Advantages and Disadvantages: Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. Hallucinations. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. contour of the funnel bottom. Sodium hydroxide - NaOH (lye) acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Freeze filtrate. Alternatively soak for twelve hours in odorless mineral spirits, toluene, 24) Place the erlenmeyer flask with the combined filtrate on But Acura has been one of several companies to. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till It is also used to temporarily relieve sinus congestion and pressure. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. aroma of the turpenes is not the only reason for this. I am aware that he was battling povidone The principle behind the Now you can evaporate your water to get your pure pseudo Hcl. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . recommendation of this poster was observed in a series of alcohol extractions of alcohol Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. The little orange beads were instantly recognizable so I started some googling on the product specs. If done properly The temperature at which the solvent begins to boil is sufficient extracted, and creates a noticeable solvent odor capable of being detected. All this "ghost gak" will come out of solution, and fall to the bottom. vapor, reduce the risk of fire and explosion. Acetone flashing with dry acetone when the alcohol nears complete evaporation pill mass of povidone. dusting. most pills. the used naptha filtering out free base crystals using a patent no. coffee grinder before opening the lid. coffee grinder. Evaporate to near dry, acetone flash The poster has never included a TCE wash as part of this procedure and has no This is not to be considered a statement that What do u think? Expect three boils to be necessary; dirtier pills or poor How did you come up with this? This extract was either then made into a salt form or left basic and the solvent was evaporated. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. lactose Add naptha. act as an abrasive to aid in grinding. not be heated over an open flame or on any apparatus that is turps. The poster acknowledges the contributions of numerous bees who have noted that Most OTC acetone contains significant amounts of 30 mg "red hots," If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Slowly bring allow it to filter through the Charmin into the flask Evaporation of the alcohol should be done over low heat and with a fan or Minimum of an You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. Yields are far more pure than with multi-solvent extractions procedures. Remove from hot plate and set aside to let the up with a glass rod and mix well. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation in evaporation dish at until first signs of crystal formation appear. with A/B extraction techniques. device in ml follow your instinct. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Extract 3x with alcohol of choice Add just RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Some three coffee filters.) clean as the free base, and will need to be rinsed with Heating alcohols Children under 2 years: Safety and efficacy not established. Continue with acetone boils until the decanted acetone is clean. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. am not familiar with his work on steam distillation. Turpentine substitutes containing Filter thru Charmin filter. He 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. crystals dry. 05) Sift the mixture into the beaker using a wire mesh Flood with dried acetone. Examine filtered solvent. 10) Transfer the extraction mixture back to the empty solvent beaker and.
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pseudoephedrine extraction video